Microscale and miniscale organic chemistry laboratory experiments

Allen M. Schoffstall, Barbara A. Gaddis, Melvin L. Druelinger

686 pages, parution le 17/09/2003 (2^eme édition)

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Résumé

This book offers a comprehensive introductory treatment of the organic laboratory techniques for handling glassware and equipment, safety in the laboratory, micro- and miniscale experimental procedures, theory of reactions and techniques, relevant background information, applications and spectroscopy.

New to This Edition

Discovery-oriented experiments. Students need to think critically and do "detective work" to investigate results that are not always a foregone conclusion.
Molecular Modeling--Exercises are provided in the text using inexpensive commercial software.
Green Chemistry--Use of indium reagents in aqueous solvents; conscious efforts to reduce quantities of toxic reagents and solvents where possible.

Features

Implements experiments early in the text that do not require spectroscopic analysis--a real benefit to most students who will not receive an introduction to IR and NMR spectroscopy until later in the course.
Introduces novel experiments, such as introductory experiments based on a discovery approach, a first semester organic qualitative analysis experiment, sequences based on heterocyclic compounds, and experiments that teach experimental design.
The book is divided into three parts: techniques, spectroscopy, and experiments. The techniques include brief experimental exercises. This organization enables students to access information effectively in the lab.

Techniques in the Organic Chemistry Laboratory
Spectroscopic Methods and Molecular Modeling
Applications Using Laboratory Resources and Techniques
Alcohols and Alkyl Halides
Synthesis of Alkenes
Alkene Addition Reactions
Molecular Modeling and Stereochemistry
Introduction to Nucleophilic Substitution Reactions
Dienes and Conjugation
Qualitative Organic Analysis I
Reactions of Aromatic Side Chains
Electrophilic Aromatic Substitution
Combined Spectroscopy and Advanced Spectroscopy
Organometallics
Alcohols and Diols
Ethers
Aldehydes and Ketones
Enols, Enolates, and Enones
Carboxylic Acids
Carboxylic Acid Esters
Dicarbonal Compounds
Amines
Aryl Halides
Phenols
Carbohydrates
Lipids
Amino Acids and Proteins
Qualitative Organic Analysis II
Projects

Caractéristiques techniques

	PAPIER
Éditeur(s)	Mc Graw Hill
Auteur(s)	Allen M. Schoffstall, Barbara A. Gaddis, Melvin L. Druelinger
Parution	17/09/2003
Édition	2^eme édition
Nb. de pages	686
Format	20,5 x 26
Couverture	Relié
Poids	1460g
Intérieur	2 couleurs
EAN13	9780071110167
ISBN13	978-0-07-111016-7