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Static Headspace-gas Chromatography

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Static Headspace-gas Chromatography

Static Headspace-gas Chromatography

Theory and Practice

Bruno Kolb, Leslie S. Ettre

350 pages, parution le 28/06/2006 (2eme édition)

Résumé

The only reference to provide both current and thorough coverage of this important analytical technique

Static headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC.

Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique. Chapters cover:

  • Principles of static and dynamic headspace analysis, including the evolution of HS-GC methods and regulatory methods using static HS-GC
  • Basic theory of headspace analysis-physicochemical relationships, sensitivity, and the principles of multiple headspace extraction
  • HS-GC techniques-vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques
  • Sample handling
  • Cryogenic HS-GC
  • Method development in HS-GC
  • Nonequilibrium static headspace analysis
  • Determination of physicochemical functions such as vapor pressures, activity coefficients, and more

Comprehensive and focused, Static Headspace-Gas Chromatography, Second Edition provides an excellent resource to help the reader achieve optimal chromatographic results. Practical examples with original data help readers to master determinations in a wide variety of areas, such as forensic, environmental, pharmaceutical, and industrial applications.

L'auteur - Bruno Kolb

Dr. Bruno Kolb is an internationally recognized expert on gas chromatography. Until his retirement in 1996, he managed the GC Applications Laboratory at Perkin-Elmer Corporation, Germany; he has also been involved in instrument development with special emphasis on specific detectors. He has been a guest lecturer at the University of Konstanz, as well as at international meetings. He has published many journal articles and book chapters, and is the author of a textbook on gas chromatography.

Sommaire

  • General introduction
  • Theoretical background of HS-GC and its applications
  • The technique of HS-GC
  • Sample handling in HS-GC
  • Headspace methods for quantitative analysis
  • Method development in HS-GC
  • Nonequilibrium static headspace analysis
  • Qualitative analysis by HS-GC
  • Special measurements
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Caractéristiques techniques

  PAPIER
Éditeur(s) Wiley
Auteur(s) Bruno Kolb, Leslie S. Ettre
Parution 28/06/2006
Édition  2eme édition
Nb. de pages 350
Format 16 x 24,5
Couverture Relié
Poids 630g
Intérieur Noir et Blanc
EAN13 9780471749448
ISBN13 978-0-471-74944-8

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