Static Headspace-gas Chromatography
Theory and Practice
Résumé
The only reference to provide both current and thorough coverage of this important analytical technique
Static headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC.
Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique. Chapters cover:
- Principles of static and dynamic headspace analysis, including the evolution of HS-GC methods and regulatory methods using static HS-GC
- Basic theory of headspace analysis-physicochemical relationships, sensitivity, and the principles of multiple headspace extraction
- HS-GC techniques-vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques
- Sample handling
- Cryogenic HS-GC
- Method development in HS-GC
- Nonequilibrium static headspace analysis
- Determination of physicochemical functions such as vapor pressures, activity coefficients, and more
Comprehensive and focused, Static Headspace-Gas Chromatography, Second Edition provides an excellent resource to help the reader achieve optimal chromatographic results. Practical examples with original data help readers to master determinations in a wide variety of areas, such as forensic, environmental, pharmaceutical, and industrial applications.
L'auteur - Bruno Kolb
Dr. Bruno Kolb is an internationally recognized expert on gas chromatography. Until his retirement in 1996, he managed the GC Applications Laboratory at Perkin-Elmer Corporation, Germany; he has also been involved in instrument development with special emphasis on specific detectors. He has been a guest lecturer at the University of Konstanz, as well as at international meetings. He has published many journal articles and book chapters, and is the author of a textbook on gas chromatography.
Sommaire
- General introduction
- Theoretical background of HS-GC and its applications
- The technique of HS-GC
- Sample handling in HS-GC
- Headspace methods for quantitative analysis
- Method development in HS-GC
- Nonequilibrium static headspace analysis
- Qualitative analysis by HS-GC
- Special measurements
Caractéristiques techniques
PAPIER | |
Éditeur(s) | Wiley |
Auteur(s) | Bruno Kolb, Leslie S. Ettre |
Parution | 28/06/2006 |
Édition | 2eme édition |
Nb. de pages | 350 |
Format | 16 x 24,5 |
Couverture | Relié |
Poids | 630g |
Intérieur | Noir et Blanc |
EAN13 | 9780471749448 |
ISBN13 | 978-0-471-74944-8 |
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